Laboratory of Materials and Chromatography Synthesis

About LSincrom


The Laboratory of Material Synthesis and Chromatography works with: catalysis, photocatalysis, synthesis of catalysts and adsorbents, fractionation, and chromatographic characterization of organic compounds present in complex matrices. The laboratory also works with the chromatographic chemical analysis of petrochemical and biofuel systems (biodiesel and bio-oil) developed chemically and enzymatically; preparation of catalysts for the production of biofuels; and preparation of photocatalysts for the degradation of pollutants in water under UV/Vis and solar radiation.

E-mail: lsincrom@itp.org.br

Phone number: +55 79 3218 2190 Telephone extension 2164



Coordination

Dra. Silvia Maria da Silva Egues
CNPq researcher Level 2
Lattes


Researchers

Dra. Laiza Canielas Krause
Lattes


Students

Juliana Faccin de Conto Borges - PhD Student
Daiane Barbosa de Matos - Doctorate Student
Jamilly Andressa Santos Barros - Doctorate Student
Kátilla Monique Costa Santos - Doctorate Student
Marília Rafaele Oliveira Santos - Doctorate Student
Mychelli Andrade Santos - Doctorate Student
Nathália Mendonça Conrado - Doctorate Student
Rafael de Oliveira Farrapeira - Doctorate Student
Ronney José Oliveira Santos - Doctorate Student
Tiago Santos Nascimento - Doctorate Student
Adriana Cerqueira Moitinho - Master Student
Luan Rodrigo Santana Silva - Master Student
Matheus Moura Oliveira - Master Student
Tamires dos Reis Menezes - Master Student
Thauane Selva Lima da Silva - Master Student
Tiago Batista Adami - Master Student
Diego da Silva Oliveira - Scientific research
Larissa Gomes Nunes - Scientific research
Tamires Nunes Faria - Scientific research
Yasmin Teles Barboza - Scientific research


Scientific production

Article -

TEIXEIRA CARDOSO, ANNE RAQUEL ; CONRADO, NATHÁLIA MENDONÇA ; KRAUSE, MAURICIO CANIELAS ; BJERK, THIAGO RODRIGUES ; Krause, Laiza Canielas ; CARAMÃO, ELINA B. . Chemical characterization of the bio-oil obtained by catalytic pyrolysis of sugarcane bagasse (industrial waste) from the species Erianthus Arundinaceus. JOURNAL OF ENVIRONMENTAL CHEMICAL ENGINEERING, v. 7, p. 102970.


Article -

SCHENA, TIAGO ; FARRAPEIRA, RAFAEL ; BJERK, THIAGO R. ; KRAUSE, LAIZA C. ; VON MÜHLEN, CARIN ; CARAMÃO, ELINA B. . Fast two-dimensional gas chromatography applied in the characterization of bio-oil from the pyrolysis of coconut fibers. Separation Science Plus, v. 1, p. 1-11.


Article -

SANTOS, KÁTILLA MONIQUE COSTA ; SANTOS, RONNEY JOSÉ OLIVEIRA ; DE ARAÚJO ALVES, MATHEUS MENDONÇA ; de Conto, Juliana Faccin ; BORGES, GUSTAVO RODRIGUES ; DARIVA, Cláudio ; EGUES, SILVIA MARIA ; SANTANA, CESAR COSTAPINTO ; FRANCESCHI, Elton . Effect of high pressure CO2 sorption on the stability of metalorganic framework MOF-177 at different temperatures. JOURNAL OF SOLID STATE CHEMISTRY, v. 269, p. 320-327.


Article -

OLIVEIRA, Ana Claudia. M. ; SANTOS, Marluce S. ; BRANDÃO, Luma M. S. ; RESENDE, Iraí T. F. ; LEO, Inmaculada M. ; MORILLO, Erika S. ; YERGA, Rufino M. N. ; FIERRO, José Luis G. ; Egues, Silvia M. S. ; FIGUEIREDO, Renan Tavares . The effect of cellulose loading on the photoactivity of cellulose-TiO 2 hybrids for hydrogen production under simulated sunlight. INTERNATIONAL JOURNAL OF HYDROGEN ENERGY, v. xx, p. 1-8.


Article -

LIMA, DAIANE ; DOS SANTOS, ANAÍ ; CELESTINO, ARIEL ; SAMPAIO, NAYNA ; BALDEZ, JÉSSICA ; MELECCHI, MARIA ; BJERK, THIAGO ; KRAUSE, LAÍZA ; CARAMÃO, ELINA . Ultrasonic Extracts of Morinda citrifolia L.: Characterization of Volatile Compounds by Gas Chromatography-Mass Spectrometry. JOURNAL OF THE BRAZILIAN CHEMICAL SOCIETY, v. 00, p. 01-08.


Article -

ZENI, Pedro F. ; SANTOS, Disley P. ; CANEVAROLO, Rafael R. ; YUNES, José Andrés ; PADILHA, Francine F. ; ALBUQUERQUE JUNIOR, Ricardo L. C. ; Egues, Silvia M. S. ; MACEDO, Maria Lucila H. . Photocatalytic and Cytotoxic Effects of Nitrogen-Doped TiO Nanoparticles on Melanoma Cells. JOURNAL OF NANOSCIENCE AND NANOTECHNOLOGY, v. 18, p. 3722-3728.


Article -

LIMA, DAIANE ; DOS SANTOS, ANAÍ ; CELESTINO, ARIEL ; SAMPAIO, NAYNA ; BALDEZ, JÉSSICA ; MELECCHI, MARIA ; BJERK, THIAGO ; KRAUSE, LAÍZA ; CARAMÃO, ELINA . Ultrasonic Extracts of Morinda citrifolia L.: Characterization of Volatile Compounds by Gas Chromatography-Mass Spectrometry. JOURNAL OF THE BRAZILIAN CHEMICAL SOCIETY, v. 00, p. 01-08.


Article -

DOS SANTOS, ANAÍ L. ; NOVAES, ANTÔNIO DA SILVA ; POLIDORO, ALLAN DOS S. ; DE BARROS, MÁRCIO EDUARDO ; MOTA, JONAS S. ; LIMA, DAIANE B.M. ; KRAUSE, LAIZA C. ; CARDOSO, CLÁUDIA A.L. ; JACQUES, ROSÂNGELA A. ; CARAMÃO, ELINA B. . Chemical characterisation of Piper amalago (Piperaceae) essential oil by comprehensive two-dimensional gas chromatography coupled with rapid-scanning quadrupole mass spectrometry (GC×GC/qMS) and their antilithiasic activity and acute toxicity. PHYTOCHEMICAL ANALYSIS, v. 1, p. 1-14.


Article -

DE JESUS, ANDERSON ALLES ; DE SANTANA SOUZA, DOMINGOS FABIANO ; DE OLIVEIRA, JACKSON ARAÚJO ; DE DEUS, MARCELL SANTANA ; DA SILVA, MAXWELL GOMES ; EGUES, Silvia Maria da Silva ; Dariva, Claudio . Mathematical modeling and experimental esterification at supercritical conditions for biodiesel production in a tubular reactor. ENERGY CONVERSION AND MANAGEMENT, v. 171, p. 1697-1703.


Article -

De Conto, Juliana Faccin ; OLIVEIRA, Marília R. ; OLIVEIRA, Matheus M. ; BRANDAO, Thadeu G. ; CAMPOS, Kelvis V. ; SANTANA, Cesar C. ; Egues, Sílvia M. . One-pot synthesis and modification of silica nanoparticles with 3-chloropropyl-trimethoxysilane assisted by microwave irradiation. CHEMICAL ENGINEERING COMMUNICATIONS, v. 205, p. 533-537.


Article -

CONTO, Juliana F. ; OLIVEIRA, Marília R. ; OLIVEIRA, Ronney J. ; CAMPOS, Kelvis V. ; MENEZES, Eliana W. ; BENVENUTTI, Edilson V. ; FRANCESCHI, Elton ; SANTANA, Cesar C. ; Egues, Silvia M. S. . Synthesis of silica modified with 1-methylimidazolium chloride by sol-gel method: A comparison between microwave radiation-assisted and conventional methods. JOURNAL OF NON-CRYSTALLINE SOLIDS, v. 1, p. 1-7.


Article -

Bispo, Mozart Daltro ; SCHNEIDER, JADERSON KLEVESTON ; DA SILVA OLIVEIRA, DIEGO ; TOMASINI, DEBORA ; DA SILVA MACIEL, GABRIELA PEREIRA ; SCHENA, TIAGO ; ONOREVOLI, BRUNA ; BJERK, THIAGO RODRIGUES ; Jacques, Rosângela Assis ; Krause, Laiza Canielas ; CARAMÃO, Elina Bastos . Production of activated biochar from coconut fiber for the removal of organic compounds from phenolic. JOURNAL OF ENVIRONMENTAL CHEMICAL ENGINEERING, v. 6, p. 2743-2750.


Article -

BARROS, JAMILLY A.S. ; KRAUSE, MAURÍCIO C. ; LAZZARI, ELIANE ; BJERK, THIAGO R. ; DO AMARAL, ADRIANE L. ; CARAMÃO, ELINA B. ; KRAUSE, LAIZA C. . Chromatographic characterization of bio-oils from fast pyrolysis of sugar cane residues (straw and bagasse) from four genotypes of the Saccharum Complex. MICROCHEMICAL JOURNAL, v. XX, p. 1-24.


Article -

Melo Junior, Carlos A. R.; ALBUQUERQUE, Carlos E. R.; Carneiro, Juliana S. A.; Dariva, Claudio; FORTUNY, Montserrat; SANTOS, Alexandre F.; Egues, Silvia M. S.; Ramos, Andre? L. D. . Solid-Acid-Catalyzed Esterification of Oleic Acid Assisted by Microwave Heating.


Article -

De Conto, Juliana Faccin; Nascimento, Juciara dos Santos; de Souza, Driele Maiara Borges; da Costa, Luiz Pereira; Egues, Silvia Maria da Silva; Freitas, Lisiane dos Santos; Benvenutti, Edilson Valmir. Solid phase extraction of petroleum carboxylic acids using a functionalized alumina as stationary phase.


Article -

JESUS, ANDERSON A.; ALMEIDA, LAYS C.; SILVA, EDSON A.; FILHO, LUCIO C.; EGUES, SILVIA M.S.; FRANCESCHI, Elton; FORTUNY, Montserrat; SANTOS, Alexandre F.; ARAUJO, JACKSON; SOUSA, ELISA M.B.D.; Dariva, Claudio. Extraction of palm oil using propane, ethanol and its mixtures as compressed solvent.


Article -

CONTO, Juliana F.; SANTOS, Marília R. O.; CARVALHO, Aiala S.; CAMPOS, Kelvis V.; FREITAS, Lisiane S.; BENVENUTTI, Edilson V.; MENEZES, Eliana W.; SANTANA, Cesar C.; Egues, Sílvia M.. Naphthenic acids recovery from petroleum using ionic silica based hybrid material as stationary phase in solid phase extraction (SPE) process.


Article -

PRADO, L.R.; DE RESENDE, N.S.; SILVA, R.S.; EGUES, S.M.S.; SALAZAR-BANDA, G.R.. Influence of the synthesis method on the preparation of barium titanate nanoparticles.


Article -

Faccini, Candice Schmitt; Cunha, Michele Espinosa da; MORAES, Maria Silvana Aranda; Krause, Laiza C.; Manique, Márcia C.; Rodrigues, Maria Regina A.; Benvenutti, Edilson V; Caramão, Elina B. Dry washing in biodiesel purification: a comparative study of adsorbents. Journal of the Brazilian Chemical Society (Impresso), v. 22, p. 558-563.


Article -

C. Cazarolli; BUCKER, F.; MANIQUE, M. C.; KRAUSE, L. C.; MACIEL, G. P. S.; Onorevoli, B.; Caramão, E. B.; CAVALCANTI, E. H. S.; SAMIOS, D.; PERALBA, M. C. R.; BENTO, F. M. Suscetibilidade do biodiesel de sebo bovino à biodegradação por Pseudallescheria boydii. Revista Brasileira de Biociências (Online), v. 10, p. 251-257.


Article -

ALMEIDA, TARCIANA MOURA; BISPO, MOZART D.; CARDOSO, ANE RAQUEL T.; MIGLIORINI, MARCELO VIEIRA; SCHENA, TIAGO; DE CAMPOS, MARIA CECÍLIA VAZ; MACHADO, MARIA ELISABETE; LÓPEZ, JORGE A.; Krause, Laíza Canielas; CARAMAO, E.B.. PRELIMINARY STUDIES OF BIO-OIL FROM FAST-PYROLYSIS OF COCONUT FIBERS. Journal of Agricultural and Food Chemistry, v. 61, p. 130619125201004-6821.


Article -

FERREIRA, DAVI DA S.; DE SOUZA COSTA, LARISSA A.; CAMPOS, MÁRCIO; BISPO, MOZART D.; Krause, Laiza C.; HERNÁNDEZ MACEDO, MARIA; LOPEZ, JORGE A. Production of xanthan gum from soybean biodiesel: a preliminary study. BMC Proceedings, v. 8, p. P174.


Article -

ONOREVOLI, BRUNA; MACHADO, MARIA ELISABETE; DARIVA, CLAUDIO; FRANCESCHI, ELTON; KRAUSE, LAÍZA C.; JACQUES, ROSÂNGELA A.; CARAMÃO, ELINA B.. A one-dimensional and comprehensive two-dimensional gas chromatography study of the oil and the bio-oil of the residual cakes from the seeds of Crambe abyssinica. Industrial Crops and Products (Print), v. 52, p. 8-16.


Article -

MACIEL, GABRIELA P. S.; MACHADO, MARIA E.; DA CUNHA, MICHELE E.; LAZZARI, ELIANE; DA SILVA, JULIANA M.; JACQUES, ROSÂNGELA A.; KRAUSE, LAIZA C.; BARROS, JAMILY A. S.; CARAMÃO, ELINA B.. Quantification of Nitrogen compounds in diesel fuel samples by comprehensive two-dimensional gas chromatography coupled with quadrupole mass spectrometry. Journal of Separation Science (Print), v. 38, p. n/a-n/a.


Article -

BISPO, M. D.; BARROS, J. A. S.; TOMASINI, D.; PRIMAZ, C.; CARAMÃO, Elina Bastos; Claudio Dariva; KRAUSE, LAIZA C.. Pyrolysis of Agroindustrial Residues of Coffee, Sugarcane Straw and Coconut-Fibers in a Semi-pilot Plant for Production of Bio-oils: Gas Chromatographic Characterization. JOURNAL OF EARTH SCIENCE AND ENGINEERING, v. 6, p. 235-244.


Article -

SILVA, JOSÉ R.O.; SANTOS, DARA S.; SANTOS, UBIRATAN R.; EGUILUZ, KATLIN I.B.; SALAZAR-BANDA, GIANCARLO R.; SCHNEIDER, JADERSON K.; KRAUSE, LAIZA C.; LÓPEZ, JORGE A.; HERNANDEZ-MACEDO, MARIA L.. Electrochemical and/or microbiological treatment of pyrolysis wastewater. CHEMOSPHERE, v. -, p. ---.


Article -

BETEMPS, GLAUCO R.; SILVEIRA, LUCAS A.; SAMPAIO, DANIELE M.; BISPO, MOZART D.; KRAUSE, LAIZA C.; CARAMÃO, ELINA B.; SANCHES FILHO, PEDRO J.; DA CUNHA, MICHELE E.. Chromatographic characterization of bio-oil generated from rapid pyrolysis of rice husk in stainless steel reactor. MICROCHEMICAL JOURNAL, v. 134, p. 218-223.